ISSN print edition: 0366-6352
ISSN electronic edition: 1336-9075
Registr. No.: MK SR 9/7
Preparation of manganese oxide nanoparticles by thermal decomposition of nanostructured manganese carbonate
Jan Pinc, Ondřej Jankovský, and Vilém Bartůněk
Department of Inorganic Chemistry, Faculty of Chemical Technology, University of Chemistry and Technology, Prague 6, Czech Republic
Abstract: MnO and Mn2O3 nanoparticles were prepared in air and argon atmosphere by thermal decomposition of nanocrystalline manganese carbonate synthesized by reaction of manganese(II) nitrate with glycerol. Samples were characterized using transmission electron microscopy, simultaneous thermal analysis and X-ray diffraction analysis. Average sizes of prepared nanoparticles were calculated from XRD patterns using Scherrer equation. Also, the conditions for decomposition of manganese carbonate were optimized to obtain optimal nanoparticle sizes. Due to suitable sizes of prepared nanoparticles and the initial material, this method can be used in a wide range of industrial applications.
Keywords: Nanoparticles; Manganese oxides; Thermal decomposition; Manganese carbonate
Full paper is available at www.springerlink.com.
Chemical Papers 71 (6) 1031–1035 (2017)