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Synthesis and characterization of 1,3,5-tris((1/2H-tetrazol-5-yl)methyl)-1,3,5-triazinane-2,4,6-trione

Yadollah Bayat and Fatemeh Hajighasemali

Department of Chemistry, School of Chemistry and Chemical Engineering, Malek-Ashtar University of Technology, Tehran, Iran

 

E-mail: y_bayat@mut.ac.ir

Abstract: 2,2′,2″-(2,4,6-Trioxo-1,3,5-triazinane-1,3,5-triyl) triacetonitrile (or tris-(cyanomethyl)-isocyanurate) and 1,3,5-tris((1/2H-tetrazol-5-yl)methyl)-1,3,5-triazinane-2,4,6-trione (or tris-(5-tetrazolylmethyl)-isocyanurate) were synthesized with new methods. High yields, simple methodology, and cheapness are advantages of the methods. Furthermore, 1,3,5-tris((1/2H-tetrazol-5-yl)methyl)-1,3,5-triazinane-2,4,6-trione was synthesized in the less hazardous condition. The compounds were characterized by elemental analysis, IR, 1HNMR, 13CNMR and mass spectroscopic analysis. In addition, DSC/TGA measurements were carried out to determine the thermal behavior of the final product.

Keywords: Isocyanuric acid; N-Alkylation; Tetrazole; Mass spectroscopy; DSC/TGA

Full paper is available at www.springerlink.com.

DOI: 10.1007/s11696-016-0018-2

 

Chemical Papers 71 (5) 949–952 (2017)

Monday, May 20, 2024

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