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Some esters of N-methyl-3-hydroxypiperidines

L. Dúbravková, I. Ježo, P. Šefčovič, and Z. Votický

Slovak Academy of Sciences, Bratislava

 

Abstract: The following CH2.NMe.CH2.CH2.CH2.CHO2CR were prepd. (R, b.p./mm., and m.p. picrate given): Me, 77-9°/15, 119-20°; Et, 92-3°/15, 140-2°; Pr, 105-10°/14, 135-7°; sec-Bu, 110-11°/15, 162-4°; MeCH:CH, 110-12°/9, 150-2°; CH2: CHCH2CHMe, 120-1°/2, -; Ph, 117-18°/0.6, 219-20° (decompn.); p-MeO-C6H4, 155°/1, 221-3° (decompn.); 3,4-(MeO)2C6H3, 168°/0.3, 213-14° (decompn.); 3,4,5-(MeO)3C6H2, 171-3°/0.5, 217-18° (decompn.); 3-pyridyl, 110-11°/0.5, 193° (decompn.); 3,4,5-(MeO)3C6H2CH:CH, -, 202-4° (decompn.).

Full paper in Portable Document Format: 107a421.pdf (in Slovak)

 

Chemical Papers 10 (7) 421–425 (1956)

Thursday, November 14, 2019

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