ISSN print edition: 0366-6352
ISSN electronic edition: 1336-9075
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Acetylation of amines with α-acetoxyacrylonitrile

J. Pokorný

Lehrstuhl für anorganische Chemie an der Chemisch-Technologischen Hochschule, Prag

 

Abstract: Exothermic reaction of α-acetoxyacrylonitrile (I) with amines was used for selective monoacetylation of amino compds. Dioxane, CHCl3, or Et2O served as solvents; a 2:1 molar ratio of amine to I was used. The reagent did not react with alc. or phenolic OH. Ethanolamine, glycine, and its derivs. were successfully acetylated.

Full paper in Portable Document Format: 183a218.pdf (in Czech)

 

Chemical Papers 18 (3) 218–221 (1964)

Tuesday, June 18, 2024

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