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Titanium(III) chlorocomplexes. I. Synthesis of the complex (TiCl3py3)

M. Zikmund, R. Foniok, and A. Valent

Slovak Academy of Sciences, Bratislava

 

Abstract: The yield of the solid complex (TiCl3py3), as a function of the molar ratio of anhyd. solid α-TiCl3 and pyridine dissolved in hexane, the pyridine concn., and the nature and time of mixing was studied. The complex was prepd. in a rotating glass reactor at 20° in an inert atm. A 98% yield was obtained after 1 hr. and by using a 3-fold excess of 1.0-1.2M pyridine soln. in hexane.

Full paper in Portable Document Format: 1911a854.pdf (in Slovak)

 

Chemical Papers 19 (11) 854–859 (1965)

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