ISSN print edition: 0366-6352
ISSN electronic edition: 1336-9075
Registr. No.: MK SR 9/7

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Detecting bis(2-chloroethyl) sulfide

V. Kratochvil and J. Martinek

Forschungsinstitut für organische Synthesen, Parclubice-Rybitvi

 

Abstract:  New, very sensitive detector tubes were developed to visualize yperite vapour in atmosphere. Tubes were tilled with 4-(4/-nitrobenzyl)pyridine complexes with mercury(II), nickel(II) and magnesium salts over purified, activated silica gel as carrier. A very high detection sensitivity has been achieved (0.5—1 μg yperite in 1 liter air). The contents of tubes being quite stable. Of detection reagents a saturated solution of sodium Perchlorate in 10% aqueous sodium hydroxide was found to be the most convenient.

Full paper in Portable Document Format: 235a382.pdf (in German)

 

Chemical Papers 23 (5) 382–390 (1969)

Thursday, October 21, 2021

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