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Alternative Syntheses of Methylated Sugars. V. Methyl Furanosides of 6-0- and 2,6-Di-O-methyl-D-glucose

P. Kováč and M. Petríková

Institute of Chemistry, Slovak Academy of Sciences, Bratislava 9

 

Abstract:  Methyl furanosides of 6-0- and 2,6-di-O-methyl-D-glucose have been synthesized. The intermediates of the synthesis were methyl 3,5-di-O-benzyl-6-0-methyl-α,ß-D-glucofuranoside and methyl 3,5-di-O-benzyl-2,6-di-0-methyl-α,ß-D-glucofuranoside which were separated into individual anomers by column chromatography on silica gel. Subsequent debenzylation of isolated compounds afforded the final products.

Full paper in Portable Document Format: 261a71.pdf

 

Chemical Papers 26 (1) 71–75 (1972)

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