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Benzothiazole compounds. XIV. Synthesis and antitubercular activity of some derivatives of N-[1-(4-R-2-benzothiazolyl-X)-2,2,2-trichloroethyl]- and N-[1-(2-X-6-R-3-benzothiazolinyl-Y)-2,2,2-trichloroethyl]formamides, -acetamides, -chloroacetamides, and -benzamides

S. Mikulášek, V. Sutoris, Ž. Odlerová, A. Perjéssy, and V. Konečný

Department of Organic Chemistry, Faculty of Natural Sciences, Komenský University, 816 31 Bratislava

 

Abstract: N-[ 1 -(4-R-2-Benzothiazolyl-X)-2,2,2-trichloroethyl]formamide, -acetamide, -chloroacetamide, and -benzamide (R = H, CI; X = 0 , SCH2 CH20) and N-[l-(2-X-6-R-3-benzothiazolinyl-Y)-2,2,2-trichloroethyl]f ormamides, -acetamide, -chloroacetamides, and -benzamide (R = H, NH2 , N02; X = O, S; Y = —, CH2CH20) were prepared by treatment of 2-mercaptobenzothiazole and some of its derivatives with N-(l,2,2,2-tetrachloroethyl)amides. Their structures were proved by interpretation of the i.r. spectra and structural changes of some compounds submitted to pyrolysis were investigated. The synthesized compounds were tested for antitubercular activity.

Full paper in Portable Document Format: 334a550.pdf

 

Chemical Papers 33 (4) 550–557 (1979)

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