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Preparation, spectral and electrochemical characterization of (dithiocarbamato)nitrosylchromium complexes

J. Labuda, J. Mocák, and D. I. Bustin

Department of Analytical Chemistry, Slovak Technical University, CS-812 37 Bratislava

 

Abstract:  Complexes of Cr[(C2H5)2iNCS2]2(H20)NO and Crr[(CH2)4NCS2]2(H20)NO were prepared. Nitrosyl coordination was verified Ы; chemical analysis and by electronic absorption, infrared, and e.p.r. spectra. Voltammetric afld cóulomet- ric characteristics were determined on platinum find dropping mercury elec- trodes in dimethylformamide and acetonitrile. Electrode reduction and oxida- tion of complexes are associated with changes, in the coordination sphere. Results were compared with conclusions drav/n from studies of analogous chromium(III) tris(dithiocarbamate) complexes;.

Full paper in Portable Document Format: 373a337.pdf

 

Chemical Papers 37 (3) 337–347 (1983)

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