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Influence of temperature, vanadium concentration, and degree of solution acidification on composition of the solid products .9. Products of the reactions taking place in acidified solutions of rubidium and cesium meta-vanadate and study of the 51V-NMR spectra of of aqueous solutions of polyvanadates

Ľ. Žurková, V. Suchá, and J. Schraml

Department of Inorganic Chemistry, Faculty of Natural Sciences, Komenský University, CS-842 15 Bratislava

 

Abstract: It has been revealed on the basis of the 51V NMR spectra of aqueous solutions of NaVO3 in acid region that the degree of their acidification and temperature influence chemical shifts, i.e. the composition of solutions. The optimum conditions of preparation of MI2V6O16 and RbHV6O16 have been determined for the systems MIVO3—HNO3—H2O (MI=Rb,Cs).

Full paper in Portable Document Format: 395a629.pdf

 

Chemical Papers 39 (5) 629–637 (1985)

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