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Estimation of nitrogen functional-groups by reaction gas-chromatography frontal technique Azoxy compounds, triazene and pentaza-1,4-diene derivatives

K. Ventura, K. Komárek, J. Churáček, H. Davidová, J. Langhans, and J. Šalamoun

Department of Analytical Chemistry,'Institute of Chemical Technology, CS-532 10 Pardubice

 

Abstract: A method of selective nitrogen determination was worked out for azoxy compounds, triazene and pentaza-l,4-diene derivatives; it is based on the destruction of the compounds in wet way with gas chromatographic deter­ mination of liberated elemental nitrogen by frontal technique. Decom­position of compounds proceeds in the apparatus placed in front of the chromatographic unit of the CHN-1 analyzer. The worked out method makes the determination of nitrogen possible in separate functional groups giving reliable and exact results and extending application possibilities of the apparatus.

Full paper in Portable Document Format: 426a773.pdf

 

Chemical Papers 42 (6) 773–780 (1988)

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