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Gas chromatography of alkyl N-phenylcarbamates

M. Šingliar, V. Macho, and J. Terlandová

Department of Organic Technology, Faculty of Chemical Technology, Slovak Technical University, CS-97104 Prievidza

 

Abstract: Methyl, ethyl, up to heptyl N-phenylcarbamates were synthesized and their retention indices were measured by gas chromatography at three column temperatures. The relationship between retention indices and number of carbon atoms in the alkyl of carbamate is linear except for the first member of the homologous series. In gas chromatographic investigations we have to take into consideration that alkyl N-phenylcarbamates and especially tert-butyl N-phenylcarbamate are thermolabile substances.

Full paper in Portable Document Format: 434a519.pdf

 

Chemical Papers 43 (4) 519–525 (1989)

Thursday, October 29, 2020

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