ISSN print edition: 0366-6352
ISSN electronic edition: 1336-9075
Registr. No.: MK SR 9/7

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Synthesis and Reactions of 5-Methoxycarbonyl-2-furylisocyanate

L. Štibrányi and J. Žúžiová

Department of Organic Chemistry, Faculty of Chemical Technology, Slovak Technical University, SK-812 31 Bratislava

 

Abstract: The synthesis of furo[3,2-e]pyrimidine-4-thione is described starting from 5-methoxy-2-furylisocyanate. The starting material is converted to substituted ureas by reaction with secondary amines. Chlorination of a urea affords chloroformamidine, which in turn cyclizes with potassium thiocyanate to give the target furopyrimidinethione.

Full paper in Portable Document Format: 506a354.pdf

 

Chemical Papers 50 (6) 354–358 (1996)

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