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Transacetalization Reaction of D-Glucuronic Acid with α,α-Dimethoxytoluene

M. Poláková and D. Joniak

Institute of Chemistry, Slovak Academy of Sciences, SK-842 38 Bratislava

 

Abstract: D-Glucuronic acid, α,α-dimethoxytoluene, and a strongly acidic cation-exchange resin in the H+ form were used in a modified transacetalization reaction. Methyl [methyl 3,5-O-benzylidene-2-O-(1-methoxybenzyl)-α-D-glucofuranosid]uronate was formed as a major product. Its structure was proved with combination of 1H  and 13C NMR spectroscopy and mass spectrometry.

Full paper in Portable Document Format: 514a230.pdf

 

Chemical Papers 51 (4) 230–233 (1997)

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